Defect and crystal structure variation in Tl-doped TlGaTe2 semiconductor alloys: An experimental and theoretical study


Abdullayev A., Samadov S. F., Abiyev A. S., Sidorin A. A., Trung N. V. M., Orlov O. S., ...More

JOURNAL OF ALLOYS AND COMPOUNDS, vol.1038, 2025 (SCI-Expanded, Scopus)

  • Publication Type: Article / Article
  • Volume: 1038
  • Publication Date: 2025
  • Doi Number: 10.1016/j.jallcom.2025.182773
  • Journal Name: JOURNAL OF ALLOYS AND COMPOUNDS
  • Journal Indexes: Science Citation Index Expanded (SCI-EXPANDED), Scopus, Chemical Abstracts Core, Chimica, Compendex, INSPEC, Public Affairs Index
  • Azerbaijan State University of Economics (UNEC) Affiliated: No

Abstract

In this work, the structural and defect characteristics of TlGaTe2 semiconductors doped with 5 % and 9 % thallium (Tl) were investigated using X-ray diffraction (XRD), positron annihilation lifetime spectroscopy (PALS), Doppler broadening spectroscopy (DBS), and first-principles calculations. XRD analysis confirmed the preservation of the tetragonal I4/mcm symmetry across all compositions, with increasing Tl content inducing local microstrain without long-range structural transitions. PALS revealed a dual defect evolution mechanism: sequential filling of micropores by Tl atoms alongside the creation of monovacancies (primarily monoGa). This was supported by the non-monotonic behavior of positron lifetime components and the ortho-positronium annihilation ratio. Electron Momentum Distribution (EMD) analysis further corroborated this, indicating Tl substitution for Ga and a modified bonding environment due to Tl occupying micropores. DBS showed a transition to a more homogeneous defect distribution with increased Tl concentration. These findings provide a detailed understanding of the complex defect dynamics induced by Tl doping in TlGaTe2, offering potential for defect engineering to tailor its properties for advanced technological applications.